ACCESSION: MSBNK-Osaka_Univ-OUF00203
RECORD_TITLE: D-Lyxose; GC-EI-TOF; MS; n TMS; RT:620.294 sec
DATE: 2016.01.19 (Created 2010.05.20, modified 2013.04.24)
AUTHORS: Tsujimoto Y, Tsugawa H, Bamba T, Fukusaki E, engineering department, Osaka Univ.
LICENSE: CC BY-SA
COMMENT: The chemical compound was chemically modified with N-methyl-N-trimethylsilyl-trifluoroacetamide (MSTFA) before GC-MS analysis. When it has two or more functional groups, this modification gave a mixture of the TMS derivatives having different number of TMS groups at different functional groups.

CH$NAME: D-Lyxose
CH$COMPOUND_CLASS: Natural Product
CH$FORMULA: C₅H₁₀O₅
CH$EXACT_MASS: 150.05282
CH$SMILES: OC(C1)C(O)C(O)C(O)O1
CH$IUPAC: InChI=1S/C5H10O5/c6-2-1-10-5(9)4(8)3(2)7/h2-9H,1H2/t2-,3+,4+,5?/m0/s1
CH$LINK: CAS 1949-78-6
CH$LINK: CHEMSPIDER 388605
CH$LINK: KEGG C01508
CH$LINK: PUBCHEM CID:439508
CH$LINK: INCHIKEY SRBFZHDQGSBBOR-AEQNFAKKSA-N
CH$LINK: COMPTOX DTXSID50331417

AC$INSTRUMENT: Pegasus III TOF-MS system, Leco; GC 6890, Agilent Technologies
AC$INSTRUMENT_TYPE: GC-EI-TOF
AC$MASS_SPECTROMETRY: MS_TYPE MS
AC$MASS_SPECTROMETRY: ION_MODE POSITIVE
AC$MASS_SPECTROMETRY: HELIUM_FLOW 1 ml/min
AC$MASS_SPECTROMETRY: ION_SOURCE_TEMPERATURE 200 C
AC$MASS_SPECTROMETRY: SCAN_RANGE_M/Z 85-500
AC$CHROMATOGRAPHY: COLUMN_NAME CP-SIL 8 CB LOW BLEED/MS
AC$CHROMATOGRAPHY: INJECTION_TEMPERATURE 230 C
AC$CHROMATOGRAPHY: OVEN_TEMPERATURE 80 C (Duration 2 min)-330 C (rate: 15 C/min; Duration 6 min)
AC$CHROMATOGRAPHY: RETENTION_INDEX 1640.916
AC$CHROMATOGRAPHY: RETENTION_TIME 620.294 sec
AC$CHROMATOGRAPHY: TRANSFARLINE_TEMPERATURE 250 C

MS$DATA_PROCESSING: WHOLE ChromaTOF ver. 2.32 (LECO)

PK$SPLASH: splash10-0uxr-0920000000-49b3e15cac5fbabcfa95
PK$NUM_PEAK: 161
PK$PEAK: m/z int. rel.int.
  85 10 10
  86 13 13
  87 15 15
  88 10 10
  89 122 122
  90 11 11
  91 6 6
  92 1 1
  93 1 1
  94 2 2
  95 1 1
  96 1 1
  97 1 1
  98 5 5
  99 10 10
  100 42 42
  101 44 44
  102 22 22
  103 999 999
  104 95 95
  105 70 70
  106 5 5
  107 2 2
  110 1 1
  111 4 4
  112 5 5
  113 12 12
  114 23 23
  115 18 18
  116 15 15
  117 106 106
  118 12 12
  119 17 17
  120 2 2
  121 1 1
  126 6 6
  127 7 7
  128 8 8
  129 90 90
  130 22 22
  131 48 48
  132 9 9
  133 123 123
  134 17 17
  135 11 11
  136 1 1
  140 3 3
  141 3 3
  142 9 9
  143 21 21
  144 4 4
  145 16 16
  146 3 3
  147 349 349
  148 56 56
  149 40 40
  150 5 5
  151 3 3
  152 1 1
  154 1 1
  155 1 1
  156 2 2
  157 8 8
  158 12 12
  159 5 5
  160 86 86
  161 21 21
  162 5 5
  163 19 19
  164 3 3
  165 2 2
  166 1 1
  168 8 8
  169 3 3
  170 2 2
  172 6 6
  173 8 8
  174 11 11
  175 12 12
  176 2 2
  177 4 4
  178 1 1
  184 2 2
  185 1 1
  186 2 2
  187 1 1
  188 1 1
  189 108 108
  190 23 23
  191 37 37
  192 6 6
  193 3 3
  198 5 5
  199 1 1
  200 4 4
  201 9 9
  202 3 3
  203 6 6
  204 34 34
  205 38 38
  206 9 9
  207 7 7
  208 1 1
  214 1 1
  215 2 2
  216 12 12
  217 398 398
  218 86 86
  219 38 38
  220 5 5
  221 9 9
  222 2 2
  223 1 1
  228 2 2
  229 1 1
  230 2 2
  231 7 7
  232 5 5
  233 27 27
  234 18 18
  235 5 5
  236 1 1
  240 1 1
  242 4 4
  243 1 1
  244 1 1
  246 2 2
  248 3 3
  256 5 5
  257 3 3
  258 2 2
  262 9 9
  263 2 2
  264 1 1
  272 2 2
  274 3 3
  275 1 1
  277 27 27
  278 11 11
  279 5 5
  280 1 1
  288 3 3
  289 1 1
  290 1 1
  291 4 4
  292 1 1
  305 2 2
  306 3 3
  307 131 131
  308 39 39
  309 20 20
  310 4 4
  311 1 1
  316 1 1
  319 1 1
  330 2 2
  331 1 1
  332 1 1
  362 2 2
  364 1 1
  467 1 1
//