ACCESSION: MSBNK-Osaka_Univ-OUF00204
RECORD_TITLE: D-Lyxose; GC-EI-TOF; MS; n TMS; RT:615.494 sec
DATE: 2016.01.19 (Created 2010.05.20, modified 2013.04.24)
AUTHORS: Tsujimoto Y, Tsugawa H, Bamba T, Fukusaki E, engineering department, Osaka Univ.
LICENSE: CC BY-SA
COMMENT: The chemical compound was chemically modified with N-methyl-N-trimethylsilyl-trifluoroacetamide (MSTFA) before GC-MS analysis. When it has two or more functional groups, this modification gave a mixture of the TMS derivatives having different number of TMS groups at different functional groups.

CH$NAME: D-Lyxose
CH$COMPOUND_CLASS: Natural Product
CH$FORMULA: C₅H₁₀O₅
CH$EXACT_MASS: 150.05282
CH$SMILES: OC(C1)C(O)C(O)C(O)O1
CH$IUPAC: InChI=1S/C5H10O5/c6-2-1-10-5(9)4(8)3(2)7/h2-9H,1H2/t2-,3+,4+,5?/m0/s1
CH$LINK: CAS 1949-78-6
CH$LINK: CHEMSPIDER 388605
CH$LINK: KEGG C01508
CH$LINK: PUBCHEM CID:439508
CH$LINK: INCHIKEY SRBFZHDQGSBBOR-AEQNFAKKSA-N
CH$LINK: COMPTOX DTXSID50331417

AC$INSTRUMENT: Pegasus III TOF-MS system, Leco; GC 6890, Agilent Technologies
AC$INSTRUMENT_TYPE: GC-EI-TOF
AC$MASS_SPECTROMETRY: MS_TYPE MS
AC$MASS_SPECTROMETRY: ION_MODE POSITIVE
AC$MASS_SPECTROMETRY: HELIUM_FLOW 1 ml/min
AC$MASS_SPECTROMETRY: ION_SOURCE_TEMPERATURE 200 C
AC$MASS_SPECTROMETRY: SCAN_RANGE_M/Z 85-500
AC$CHROMATOGRAPHY: COLUMN_NAME CP-SIL 8 CB LOW BLEED/MS
AC$CHROMATOGRAPHY: INJECTION_TEMPERATURE 230 C
AC$CHROMATOGRAPHY: OVEN_TEMPERATURE 80 C (Duration 2 min)-330 C (rate: 15 C/min; Duration 6 min)
AC$CHROMATOGRAPHY: RETENTION_INDEX 1630.470
AC$CHROMATOGRAPHY: RETENTION_TIME 615.494 sec
AC$CHROMATOGRAPHY: TRANSFARLINE_TEMPERATURE 250 C

MS$DATA_PROCESSING: WHOLE ChromaTOF ver. 2.32 (LECO)

PK$SPLASH: splash10-0udi-0920000000-4ed80ea04c978215cb32
PK$NUM_PEAK: 132
PK$PEAK: m/z int. rel.int.
  85 9 9
  86 7 7
  87 14 14
  88 10 10
  89 156 156
  90 14 14
  91 7 7
  94 1 1
  98 4 4
  99 11 11
  100 57 57
  101 42 42
  102 24 24
  103 999 999
  104 97 97
  105 62 62
  106 3 3
  107 1 1
  109 1 1
  111 4 4
  112 4 4
  113 9 9
  114 9 9
  115 11 11
  116 12 12
  117 112 112
  118 12 12
  119 19 19
  120 1 1
  121 1 1
  126 6 6
  127 5 5
  128 4 4
  129 109 109
  130 24 24
  131 52 52
  132 10 10
  133 126 126
  134 18 18
  135 13 13
  140 3 3
  141 1 1
  142 5 5
  143 18 18
  144 3 3
  145 12 12
  146 2 2
  147 338 338
  148 56 56
  149 37 37
  150 5 5
  151 1 1
  152 1 1
  154 1 1
  156 1 1
  157 12 12
  158 8 8
  159 5 5
  160 74 74
  161 24 24
  162 6 6
  163 17 17
  164 3 3
  165 1 1
  168 2 2
  171 1 1
  172 6 6
  173 7 7
  174 13 13
  175 13 13
  176 2 2
  177 6 6
  184 1 1
  188 3 3
  189 119 119
  190 24 24
  191 34 34
  192 6 6
  193 3 3
  200 4 4
  201 7 7
  202 2 2
  203 8 8
  204 29 29
  205 41 41
  206 8 8
  207 8 8
  208 1 1
  214 3 3
  215 1 1
  216 3 3
  217 380 380
  218 81 81
  219 39 39
  220 6 6
  221 11 11
  222 2 2
  223 1 1
  229 1 1
  230 1 1
  231 6 6
  232 5 5
  233 36 36
  234 10 10
  235 5 5
  238 1 1
  240 1 1
  241 1 1
  247 1 1
  248 3 3
  256 5 5
  257 1 1
  258 1 1
  261 1 1
  262 9 9
  263 2 2
  274 2 2
  275 1 1
  277 30 30
  278 12 12
  279 5 5
  280 2 2
  291 4 4
  292 1 1
  305 1 1
  306 2 2
  307 119 119
  308 38 38
  309 19 19
  310 4 4
  320 1 1
  467 1 1
//