MassBank Record: MSBNK-Fac_Eng_Univ_Tokyo-JP005456
ACCESSION: MSBNK-Fac_Eng_Univ_Tokyo-JP005456
RECORD_TITLE: (4R*,5R*,6R*)-4-(ETHOXYCARBONYL)METHYL-5-(TRIETHYLSILYL)OXY-6-METHYLPERHYDRO-1,3-OXAZINE-2-ONE; EI-B; MS
DATE: 2016.01.19 (Created 2008.10.21, modified 2011.05.06)
AUTHORS: HIRAMA M, TOHOKU UNIV. FACULTY OF SCIENCE DEPT. OF CHEMISTRY YUKIBUNSEKI
LICENSE: CC BY-NC-SA
CH$NAME: (4R*,5R*,6R*)-4-(ETHOXYCARBONYL)METHYL-5-(TRIETHYLSILYL)OXY-6-METHYLPERHYDRO-1,3-OXAZINE-2-ONE
CH$COMPOUND_CLASS: N/A
CH$FORMULA: C15H29NO5Si
CH$EXACT_MASS: 331.1815
CH$SMILES: N/A
CH$IUPAC: N/A
AC$INSTRUMENT: HITACHI M-52
AC$INSTRUMENT_TYPE: EI-B
AC$MASS_SPECTROMETRY: MS_TYPE MS
AC$MASS_SPECTROMETRY: ION_MODE POSITIVE
AC$MASS_SPECTROMETRY: IONIZATION_ENERGY 14 eV
MS$FOCUSED_ION: ION_TYPE [M]+*
PK$SPLASH: splash10-0udi-0795000000-01b2a76908fb2da042d4
PK$NUM_PEAK: 101
PK$PEAK: m/z int. rel.int.
18 3.3 33
43 1.3 13
57 4.2 42
70 0.47 5
71 0.9 9
72 1 10
73 1.1 11
83 0.08 1
84 3.7 37
85 0.7 7
87 1 10
89 0.14 1
96 1.3 13
97 0.8 8
99 1.7 17
100 0.07 1
102 2.6 26
103 13 130
110 6.7 67
111 0.47 5
112 9.9 99
113 14.3 143
114 1 10
115 0.3 3
116 5.3 53
119 1.2 12
123 1.3 13
127 0.14 1
130 2.2 22
131 4.9 49
138 1 10
141 0.22 2
142 1.7 17
143 4.4 44
144 2.1 21
145 0.22 2
146 1.1 11
147 2.2 22
149 42.2 422
150 0.65 7
154 2.4 24
157 1.2 12
158 1 10
167 2 20
168 1.7 17
169 5.6 56
170 17 170
171 0.38 4
172 21 210
173 10.7 107
174 5.5 55
175 0.06 1
181 2.6 26
182 1.1 11
183 1.7 17
184 0.29 3
185 6 60
186 9.7 97
187 0.8 8
199 0.59 6
200 2.8 28
210 2 20
211 0.7 7
212 0.37 4
213 45.6 456
214 13 130
215 4 40
216 0.17 2
217 3.2 32
218 1 10
222 1 10
228 0.35 4
230 1.7 17
231 1.1 11
232 0.7 7
241 0.58 6
242 3 30
245 1.1 11
256 36.6 366
257 1.3 13
258 6.4 64
259 32.2 322
260 13.1 131
261 0.6 6
262 0.7 7
266 1.3 13
274 3.6 36
275 0.09 1
279 41.8 418
280 8.8 88
281 2.9 29
284 0.48 5
285 1.7 17
286 6 60
287 0.6 6
300 0.23 2
302 99.99 999
303 31.9 319
304 23.6 236
305 0.45 5
332 1.9 19
//
